1197040-29-1合成路线 （共 99 条）
反应条件
(i) Me2NCH2CH2NMe2, Et2O, (ii) SCl2; Multistep reaction;
参考文献
Walborsky,H.M.; Ronman,P.
Journal of Organic Chemistry, 1978 , vol. 43, # 4 p. 731 - 734
反应条件
hexamethyl-distannane in benzene
1.5 h; Photolysis;
参考文献
Gabarda, Ana E; Du, Wu; Isarno, Thomas; Tangirala, Raghuram S; Curran, Dennis P
Tetrahedron, 2002 , vol. 58, # 32 p. 6329 - 6341
参考文献
Pawlewski
Chemische Berichte, 1899 , vol. 32, p. 1426
反应条件
1: pyridine With fluorine in chloroform
T=-78 - -60°C;
2: phenyl isocyanate With trimethylsilylazide in chloroform
T=-50 - 0°C;
参考文献
Kiselyov, Alexander S.
Tetrahedron Letters, 2005 , vol. 46, # 29 p. 4851 - 4854
反应条件
bromine
1.) 5 deg C, 0.5 h, 2.) RT, 5 h;
参考文献
Yamada, Hideyo; Wada, Yasuo; Tanimoto, Shigeo; Okano, Masaya
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 8 p. 2480 - 2483
反应条件
titanium tetrachloride
1.) dichloromethane, 0 deg C, 60 min; 2.) dichloromethane0 deg C; Yield given. Multistep reaction;
参考文献
Seebach, Dieter; Adam, Geo; Gees, Thomas; Schiess, Martin; Weigand, Wolfgang
Chemische Berichte, 1988 , vol. 121, p. 507 - 518
反应条件
hexamethyl-distannane in benzene
T=85°C; Irradiation;
参考文献
Curran, Dennis P.; Liu, Hui; Josien, Hubert; Ko, Sung-Bo
Tetrahedron, 1996 , vol. 52, # 35 p. 11385 - 11404
反应条件
hexamethyl-distannane in benzene
T=85°C; Irradiation;
参考文献
Curran, Dennis P.; Liu, Hui; Josien, Hubert; Ko, Sung-Bo
Tetrahedron, 1996 , vol. 52, # 35 p. 11385 - 11404
反应条件
in ammonia
react. in liq. NH3 at -33 - -40 °C;;
参考文献
Nast, R.; Schulz, H.; Moerler, H.-D.
Chemische Berichte, 1970 , vol. 103, p. 777 - 784
Full Text Show Details
Gmelin Handbook: Ni: Org.Verb.1, 1.1.6.4.1, page 327 - 333
参考文献
Klages, F.; Moenkemeyer, K.
Naturwissenschaften, 1950 , vol. 37, p. 210 - 210
