1197040-29-1合成路线 （共 99 条）
反应条件
in toluene
all manipulations under Ar atm.; soln. of isocyanide added to soln. of Ni compd. over period of 1 h at room temp.; concd., cooled to -10°C, after 24 h filtered; elem. anal.;
参考文献
Hahn, F. Ekkehardt; Muender, Marco; Froehlich, Roland
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2004 , vol. 59, # 8 p. 850 - 854
反应条件
hydrazine hydrate in ethanol
addn. of hydrazine hydrate and 10percent alc. KOH-soln. to soln. of C6H5NC in ethanol, dropwise addn. of Ni(CH3CO2)2 with stirring;; pptn., washing with alc.;;
参考文献
Gmelin Handbook: Ni: MVol.C1, 1, page 2 - 9
反应条件
react. of C6H5NC with (Ni(CO)(P(OC2H5)3)3);;
参考文献
Gmelin Handbook: Ni: MVol.B3, 29, page 829 - 831
反应条件
byproducts: CO; prepn. from (CO)3NiC(CH3)2P(C6H5)3 and 11-fold excess of C6H5NC;;
参考文献
Gmelin Handbook: Ni: Org.Verb.1, 1.1.6.4.1, page 327 - 333
反应条件
in diethyl ether
<O°C;
参考文献
Gmelin Handbook: Ni: Org.Verb.2, 1.5.2.1.3, page 204 - 210
参考文献
Baker, R.; Cookson, R. C.; Vinson, J. R.
J. Chem. soc. Chem. Comun., 1974 , p. 515 - 516
反应条件
carbon monoxide
between -40 and -60°C;
参考文献
Gmelin Handbook: Ni: Org.Verb.2, 1.6.1.2, page 225 - 243
反应条件
byproducts: (C6H5)3P; react. with C6H5NC;;
参考文献
Gmelin Handbook: Ni: Org.Verb.1, 1.1.5.3.2.8, page 182 - 185
反应条件
hexamethyl-distannane in various solvent(s)
T=150°C; 48 h; Irradiation;
参考文献
Camaggi, Carlo Maurizio; Leardini, Rino; Nanni, Daniele; Zanardi, Giuseppe
Tetrahedron, 1998 , vol. 54, # 21 p. 5587 - 5598
参考文献
Saegusa,T. et al.
Synthetic Communications, 1971 , vol. 1, p. 145 - 152
