1197040-29-1合成路线 （共 99 条）
参考文献
Passerini
Gazzetta Chimica Italiana, 1922 , vol. 52 II, p. 256
反应条件
potassium iodide in dimethyl sulfoxide
4 h;
参考文献
Russell, Glen A.; Rajaratnam, Ragine; Chen, Ping
Acta Chemica Scandinavica, 1998 , vol. 52, # 5 p. 528 - 532
反应条件
1: With pyridine 1-oxide; tetrachlorosilane in dichloromethane
T=-74°C; 4 h;
2: With sodium hydrogencarbonate in dichloromethane
T=20°C; 2 h;
参考文献
Denmark, Scott E.; Fan, Yu
Journal of the American Chemical Society, 2003 , vol. 125, # 26 p. 7825 - 7827
反应条件
1: pyridine N-oxide; SiCl4 / CH2Cl2 / 4 h / -74 °C
2: 173 mg / NaHCO3 / H2O; CH2Cl2 / 2 h / 20 °C
View Scheme
参考文献
Passerini
Gazzetta Chimica Italiana, 1924 , vol. 54, p. 534
反应条件
sodium tris(acetoxy)borohydride
T=-40 - 0°C; 7 h; Further byproducts given;
参考文献
Kiselyov, Alexander S.
Tetrahedron Letters, 2005 , vol. 46, # 26 p. 4487 - 4490
反应条件
NSC26899; [Ru(II)(2,2’-bipyridine)3]Cl2 in water; tert-butyl alcohol
T=80°C; 12 h; Irradiation;
参考文献
Curran, Dennis P.; Liu, Hui; Josien, Hubert; Ko, Sung-Bo
Tetrahedron, 1996 , vol. 52, # 35 p. 11385 - 11404
反应条件
hexamethyl-distannane in various solvent(s)
T=150°C; 38 h; Irradiation;
参考文献
Curran, Dennis P.; Liu, Hui
Journal of the American Chemical Society, 1991 , vol. 113, # 6 p. 2127 - 2132
反应条件
1: 2.) TMEDA / 1.) ether, -78 deg C, 15 min; 2.) below 0 deg C, then r.t., 6 h
2: 55 percent / diethyl ether / 15 h / Ambient temperature
3: 600 °C / 0.01 Torr
View Scheme
参考文献
Heinicke, Joachim
Journal of Organometallic Chemistry, 1989 , vol. 364, p. C17 - C21
反应条件
(i) Me2NCH2CH2NMe2, Et2O, (ii) /BRN= 609882/; Multistep reaction;
参考文献
Walborsky,H.M.; Ronman,P.
Journal of Organic Chemistry, 1978 , vol. 43, # 4 p. 731 - 734
反应条件
(i) Me2NCH2CH2NMe2, Et2O, (ii) /BRN= 508189/; Multistep reaction;
参考文献
Walborsky,H.M.; Ronman,P.
Journal of Organic Chemistry, 1978 , vol. 43, # 4 p. 731 - 734
