1,2-二氯-3,4,5,6-四氟苯合成路线 (共 2 条)
反应条件
para-dichlorobenzene; 1,3-dichloro-2,4,5,6-tetrafluorobenzene; phosphorous acid trisdiethylamide in hexane
T=20°C; Reduction; silyldehalogenation; 168 h; Title compound not separated from byproducts;
参考文献
Bardin
Russian Chemical Bulletin, 1997 , vol. 46, # 4 p. 780 - 785
反应条件
sodium methylate in methanol
T=-7.6°C; Rate constant;
参考文献
Chambers, Richard D.; Close, Deborah
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 778 - 780