2,2-二氟-1,3-苯并二恶茂-4-甲醛合成路线 （共 8 条）
反应条件
sec.-butyllithium in tetrahydrofuran; cyclohexane T=-75°C;
参考文献
Schlosser, Manfred; Gorecka, Joanna; Castagnetti, Eva
European Journal of Organic Chemistry, 2003 , # 3 p. 452 - 462
反应条件
hydrogenchloride in water
反应条件
hydrogenchloride in acetic acid
反应条件
1: 95 percent / sodium borohydride / methanol / 0.25 h / 0 °C 2: 89 percent / potassium hydroxide / diethyl ether; H2O / 15 h / 25 °C 3: 71 percent / 18-crown-6 / acetonitrile / 20 h / Heating View Scheme
参考文献
Schlosser, Manfred; Gorecka, Joanna; Castagnetti, Eva
European Journal of Organic Chemistry, 2003 , # 3 p. 452 - 462
反应条件
sodium tetrahydroborate in methanol T=0°C; 0.25 h;
参考文献
Schlosser, Manfred; Gorecka, Joanna; Castagnetti, Eva
European Journal of Organic Chemistry, 2003 , # 3 p. 452 - 462
反应条件
ammonia; iodine in tetrahydrofuran; water T=25°C; 2 h;
参考文献
Schlosser, Manfred; Gorecka, Joanna; Castagnetti, Eva
European Journal of Organic Chemistry, 2003 , # 3 p. 452 - 462
反应条件
1: 95 percent / sodium borohydride / methanol / 0.25 h / 0 °C
2: 86 percent / triphenylphosphane; bromine / acetonitrile / 2 h / 50 °C
View Scheme
参考文献
Schlosser, Manfred; Gorecka, Joanna; Castagnetti, Eva
European Journal of Organic Chemistry, 2003 , # 3 p. 452 - 462
