3-甲基-5-苯基-1,2,4-噁二唑合成路线 （共 19 条）
参考文献
Smith, Richard F.; Coffman, Karen J.; Geer, Susan M.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 69 - 71
反应条件
1: 69 percent / iPr2NEt / CH2Cl2 / 1 h / 0 °C
2: 90 percent / n-Bu4NF / tetrahydrofuran / 48 h / 23 °C
View Scheme
参考文献
Gangloff, Anthony R.; Litvak, Joane; Shelton, Emma J.; Sperandio, David; Wang, Vivian R.; Rice, Kenneth D.
Tetrahedron Letters, 2001 , vol. 42, # 8 p. 1441 - 1443
反应条件
hydroxylamine in methanol
Heating;
参考文献
Baccar,B.-G.; Mathis,F.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1965 , vol. 261, p. 174 - 177
反应条件
in toluene
T=110°C; 0.5 h;
参考文献
Videtta, Valeria; Perrone, Serena; Rosato, Francesca; Alifano, Pietro; Tredici, Salvatore M.; Troisi, Luigino
Synlett, 2010 , # 18 p. 2781 - 2783
反应条件
sodium carbonate in ethanol
Heating;
参考文献
Weidinger,H.; Kranz,J.
Chemische Berichte, 1963 , vol. 96, p. 1049 - 1058
反应条件
phenyl isocyanate; triethylamine in benzene
参考文献
Micetich,R.G.
Canadian Journal of Chemistry, 1970 , vol. 48, p. 2006 - 2015
反应条件
(i) NaOCl, aq. HCl, MeOH, (ii) aq. Na2CO3; Multistep reaction;
参考文献
Goetz,N.; Zeeh,B.
Synthesis, 1976 , p. 268 - 270
反应条件
in acetonitrile
48 h; also in the presence of 2,6-di-tert-butyl-4-methylpyridine (before, 1h after or 12 h after reaction had been started); Product distributionMechanism;
参考文献
Chiou, Shishue; Hoque, A. K. M. M.; Shine, Henry J.
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3227 - 3232
反应条件
oxygen in acetonitrile
4 h; Irradiation;
参考文献
Palumbo Piccionello, Antonio; Pibiri, Ivana; Pace, Andrea; Raccuglia, Rosa Angela; Buscemi, Silvestre; Vivona, Nicolo; Giorgi, Gianluca
Heterocycles, 2007 , vol. 71, # 7 p. 1529 - 1537
