反应条件
sodium in diethyl ether byproducts: sodium phenylacetylenide; the soln. of stannane was added dropwise to a suspn. of Na, the mixt. was stirred with light boiling of ether until sodium completely consumed to give acetylenide (2-3 h), filtered under N2; the product was sepd. from filtrate by distn.;
参考文献
Komarov, N. V.; Andreev, A. A.; Shein, O. G.
Russian Chemical Bulletin, 1994 , vol. 43, # 6 p. 1048 - 1049
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1994 , # 6 p. 1109 - 1110
