aluminium trichloride in dichloromethane 3 h; Ambient temperature;
参考文献
Kashin, A. N.; Bumagin, N. A.; Kalinovskii, I. O.; Beletskaya, I. P.; Reutov, O. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 7 p. 1329 - 1334
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 7 p. 1569 - 1575
in further solvent(s) Irradiation (UV/VIS); heating a mixt. of 0.02 mole Me3SnCCPh and 0.17 mole CF3I to 90°C and UV irradn. in a sealed tube; removal of excess CF3I, distn. under reduced pressure;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 56, p. 1474 - 1475
Zhurnal Obshchei Khimii, , vol. 56, p. 1663 - 1663
catalyst: a palladium complex in 1,2-dichloro-ethane 100°C, 3 h, sealed glass ampul purged with argon; molar ratio of stannaalkene:stannaalkyne=1:1 and a deficiency of C3F7I; proportion of C3F7CHCHC6H5 : C3F7CCC6H5 = 3 : 1;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 59, p. 1620 - 1624
Zhurnal Obshchei Khimii, , vol. 59, p. 1818 - 1823
tetrakis(triphenylphosphine) palladium(0) in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; 6 h;
参考文献
Bumagin, N. A.; Kasatkin, A. N.; Beletskaya, I. P.
Doklady Chemistry, 1982 , vol. 266, p. 345 - 348
Dokl. Akad. Nauk SSSR Ser. Khim., 1982 , vol. 266, # 4 p. 862 - 866