1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane 0.5 h; Yield given;
参考文献
Dziadulewicz, Edward; Hodgson, David; Gallagher, Timothy
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3367 - 3374
Multi-step reaction with 2 steps 1: 1,8-diazabicyclo<5.4.0>undec-7-ene / CH2Cl2 / 0.5 h2: 1.) LDA / 1.) THF, -78 to -40 deg C, 1.5 h then -40 deg C, 30 min, 2.) THF, -78 deg C
参考文献
Dziadulewicz, Edward; Hodgson, David; Gallagher, Timothy Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3367 - 3374
