6-溴-1,1,4,4,7-五甲基-1,2,3,4-四氢萘合成路线 （共 14 条）
反应条件
1: n-BuLi / tetrahydrofuran; hexane / 3 h / -78 - 20 °C 2: 2.38 g / aq. HCl / tetrahydrofuran / 2 h / 20 °C 3: 88 percent / Pd(OAc)2; P(o-Tol)3; Et3N / dimethylformamide / 2 h / 50 °C View Scheme
参考文献
Faul; Ratz; Sullivan; Trankle; Winneroski
Journal of Organic Chemistry, 2001 , vol. 66, # 17 p. 5772 - 5782
反应条件
1: n-BuLi / tetrahydrofuran; hexane / 3 h / -78 - 20 °C 2: 2.38 g / aq. HCl / tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 66, # 17 p. 5772 - 5782
反应条件
hydrogenchloride; n-butyllithium in tetrahydrofuran; hexane
反应条件
1: n-BuLi / tetrahydrofuran; hexane / 3 h / -78 - 20 °C 2: 2.38 g / aq. HCl / tetrahydrofuran / 2 h / 20 °C 3: 88 percent / Pd(OAc)2; P(o-Tol)3; Et3N / dimethylformamide / 2 h / 50 °C 4: H2O View Scheme
参考文献
Zou, Yinjun; Qin, Liena; Ren, Xinfeng; Lu, Yunpeng; Li, Yongxin; Zhou, Jianrong
Chemistry - A European Journal, 2013 , vol. 19, # 10 p. 3504 - 3511
