2-(4-甲基苯)苯并咪唑合成路线 （共 56 条）
反应条件
silphox [POCl3-n(SiO2)n, silica phosphinoxide] in N,N-dimethyl-formamide
0.133333 h; Microwave irradiation;
参考文献
Rambabu; Murthi, P. Radha Krishna; Dulla, Balakrishna; Basaveswara Rao; Pal, Manojit
Synthetic Communications, 2013 , vol. 43, # 22 p. 3083 - 3092
反应条件
hydrogenchloride; dihydrogen peroxide in acetonitrile
T=20°C; 0.583333 h;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad Mehdi; Naali, Fardin
Synlett, 2009 , # 4 p. 569 - 572
反应条件
exo/endo-9-cyclohexyl-9-phospabicyclo[4.2.1]nonane; isobutyldiisopropylamine; [RhCl(cis-cyclooctene)2]2 in 1,2-dichloro-benzene
T=250°C; 0.666667 h; microwave irradation;
参考文献
Lewis, Jared C.; Wu, Jessica Y.; Bergman, Robert G.; Ellman, Jonathan A.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 10 p. 1589 - 1591
反应条件
sulfur in neat (no solvent)
T=130°C; 20 h; Inert atmosphere;
参考文献
Nguyen, Thanh Binh; Ermolenko, Ludmila; Dean, William A.; Al-Mourabit, Ali
Organic Letters, 2012 , vol. 14, # 23 p. 5948 - 5951
反应条件
2,6-dimethylpyridine; bis(triphenylphosphine)palladium(II)-chloride in N,N-dimethyl acetamide
T=140°C; P=4912.9 Torr; 24 h;
参考文献
Perry; Wilson
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7016 - 7021
反应条件
copper(I) oxide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl-formamide
T=140°C; 16 h; Inert atmosphere;
参考文献
Qu, Yanyang; Pan, Lei; Wu, Zhiqing; Zhou, Xiangge
Tetrahedron, 2013 , vol. 69, # 6 p. 1717 - 1719
反应条件
oxygen; scandium tris(trifluoromethanesulfonate) in tetrahydrofuran
T=20°C; 44 h;
参考文献
Itoh, Takashi; Nagata, Kazuhiro; Ishikawa, Hiroyuki; Ohsawa, Akio
Heterocycles, 2004 , vol. 63, # 12 p. 2769 - 2783
反应条件
sodium dithionite in water; N,N-dimethyl-formamide
microwave irradiation;
参考文献
Surpur, Mandar P.; Singh, Pankajkumar R.; Patil, Sachin B.; Samant, Shriniwas D.
Synthetic Communications, 2007 , vol. 37, # 8 p. 1375 - 1379
反应条件
copper(I) oxide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl-formamide
T=140°C; 16 h; Inert atmosphere;
参考文献
Qu, Yanyang; Pan, Lei; Wu, Zhiqing; Zhou, Xiangge
Tetrahedron, 2013 , vol. 69, # 6 p. 1717 - 1719
反应条件
1: (4-methylphenyl)methyl alcohol With iodine; potassium carbonate in tert-butyl alcohol
T=50°C; 2 h;
2: 1,2-diamino-benzene in tert-butyl alcohol
T=70°C; 3 h; Further stages.;
参考文献
Ren, Yi-Ming; Cai, Chun
Organic Preparations and Procedures International, 2008 , vol. 40, # 1 p. 101 - 105
