反应条件
1.1: trichlorophosphate / 1,2-dichloro-ethane / 0.17 h / 0 °C
1.2: 3 h / Reflux
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere
2.2: 1.5 h / 20 °C / Inert atmosphere
3.1: palladium 10 on activated carbon; hydrogen / ethyl acetate / 1.5 h / 20 °C
4.1: hydrogenchloride / 4 h / 100 °C
View Scheme
参考文献
Khunnawutmanotham, Nisachon; Chimnoi, Nitirat; Champathong, Wattanachai; Lerdsirisuk, Pradit; Khotmor, Theeraphon; Techasakul, Supanna
Journal of Chemical Research, 2012 , vol. 36, # 6 p. 374 - 378