3,4-二甲氧基苯甲醛合成路线 (共 996 条)
反应条件
water; TiF4 T=60°C; 1.3 h; screw-capped vial;
参考文献
Jung, Misuk; Yoon, Jieun; Kim, Hak Sung; Ryu, Jae-Sang
Synthesis, 2010 , # 16 art. no. F04310SS, p. 2713 - 2720
反应条件
1: vanillin With potassium carbonate in acetone T=40 - 45°C; 1 h; Inert atmosphere; 2: methyl iodide in acetone 7 h; RefluxInert atmosphere;
参考文献
Alves, Ana P. L.; Junior, Jose Augusto B. C.; Slana, Glaucia B. A.; Cardoso, Jari N.; Wang, Qiang; Lopes, Rosangela S. C.; Lopes, Claudio C.
Synthetic Communications, 2009 , vol. 39, # 20 p. 3693 - 3709
反应条件
polymer supported perruthenate reagent in dichloromethane
参考文献
Hajipour, Abdol R.; Mallakpour, Shadpour E.; Malakoutikhah, Morteza
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 1 p. 195 - 198
反应条件
laccase from Trametes versicolor; oxygen; benzotriazol-1-ol in water T=45°C; 22 h; pH=4.5;
参考文献
Fritz-Langhals, Elke; Kunath, Brigitte
Tetrahedron Letters, 1998 , vol. 39, # 33 p. 5955 - 5956
反应条件
water; phosphorus pentoxide 0.0222222 h; microwave irradiation;
参考文献
Banerjee, Krishna; Mitra, Alok Kumar
Journal of the Indian Chemical Society, 2003 , vol. 80, # 3 p. 184 - 186
反应条件
water; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione T=50°C; 0.5 h; Ionic liquidInert atmosphere;
参考文献
Dake, Satish A.; Kulkarni, Ravibhushan S.; Rode, Ambadas B.; Shinde, Pravin S.; Ghumbre, Sushil K.; Magar, Rupali L.; Pawar, Rajendra P.
Letters in Organic Chemistry, 2010 , vol. 7, # 6 p. 491 - 494
反应条件
potassium carbonate in acetone T=20°C; 1.5 h; Reflux;
参考文献
Gavara, Laurent; Boisse, Thomas; Henichart, Jean-Pierre; Daich, Adam; Rigo, Benoit; Gautret, Philippe
Tetrahedron, 2010 , vol. 66, # 38 p. 7544 - 7561
反应条件
AgNO2; iodine in tetrahydrofuran 1.5 h; Ambient temperature;
参考文献
Nishide, Kiyoharu; Yokota, Kouichi; Nakamura, Daisaku; Sumiya, Toshio; Node, Manabu; Ueda, Masaru; Fuji, Kaoru
Tetrahedron Letters, 1993 , vol. 34, # 21 p. 3425 - 3428
反应条件
potassium dichromate; aluminium trichloride 0.0333333 h;
参考文献
Mohammadpoor-Baltork, Iraj; Sadeghi, Majid M.; Adibi, Abol-Hassan
Molecules, 2001 , vol. 6, # 11 p. 900 - 908
反应条件
perchloric acid in methanol; water T=25 - 30°C; 0.166667 h;
参考文献
Kumar, Dinesh; Kumar, Raj; Chakraborti, Asit K.
Synthesis, 2008 , # 8 p. 1249 - 1256