3,4-二甲氧基苯甲醛合成路线 (共 996 条)
反应条件
in water; acetonitrile T=40°C;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 5 p. 891 - 896
反应条件
sodium perchlorate in acetonitrile anode potential 0.95 - 1.1 V;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 833 - 837
反应条件
hydrogenchloride in methanol 13 h; Irradiation;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2059 - 2064
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane a) 0 deg C, 30 min, b) from 0 deg C to RT;
参考文献
Kasum, Bruno; Prager, Rolf H.
Australian Journal of Chemistry, 1983 , vol. 36, # 7 p. 1455 - 1467
反应条件
lignin peroxidase; dihydrogen peroxide; disodium 2,3-dihydroxysuccinate in water; acetonitrile T=25°C; pH=4.0; 1 h;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 9 p. 1506 - 1511
反应条件
1: NaBH4 / methanol / 2 h / Ambient temperature 2: 50 percent / Pb(OAc)4 / CH2Cl2 / Ambient temperature View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 115, # 1 p. 7 - 12
反应条件
1: aq. ethanol / 0.25 h / Ambient temperature 2: 1.) sodium hydride / 1.) THF, 1.5 h, 2.) 15 min 3: 73.8 percent / acetone / 69 h / Heating 4: methanol / 0.25 h / Irradiation View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2059 - 2064
反应条件
1: 1.) sodium hydride / 1.) THF, 1.5 h, 2.) 15 min 2: 73.8 percent / acetone / 69 h / Heating 3: methanol / 0.25 h / Irradiation View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2059 - 2064
反应条件
1: 61 percent / 2M HCl, sodium nitrite / aq. ethanol; H2O / 0.42 h / 20 - 60 °C 2: 10 mg / conc. HCl / methanol / 13 h / Irradiation View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2059 - 2064
反应条件
1: 57 percent / sodium borohydride / ethanol / 0.75 h 2: 1.) sodium hydride / 1.) THF, 1.5 h, 2.) 15 min 3: 73.8 percent / acetone / 69 h / Heating 4: methanol / 0.25 h / Irradiation View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2059 - 2064