3,4-二甲氧基苯甲醛合成路线 （共 996 条）
反应条件
1: 2.) 55percent aq. HI / 1.) aq. ethanol, 0 deg C, 20 min, 2.) ethanol 2: 57 percent / sodium borohydride / ethanol / 0.75 h 3: 1.) sodium hydride / 1.) THF, 1.5 h, 2.) 15 min 4: 73.8 percent / acetone / 69 h / Heating 5: methanol / 0.25 h / Irradiation View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2059 - 2064
反应条件
1: K2S2O8, AgNO3 / H2O; acetonitrile / 40 °C 2: H2O; acetonitrile / 40 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 5 p. 891 - 896
反应条件
1.1: isopropylmagnesium chloride / tetrahydrofuran / 1.33 h / -25 °C 1.2: 1.33 h / -75 °C 2.1: dichloromethane / 48 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 70, # 3 p. 643 - 649
反应条件
sodium perchlorate in acetonitrile anode potential 1.0 - 1.1 V;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 833 - 837
反应条件
dihydrogen peroxide; acetic acid; methyltrioxorhenium(VII) on poly(4-vinylpyridine) T=20°C; 6 h; Product distribution; Further Variations:Catalysts;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 14, # 15 p. 5292 - 5302
反应条件
water; sodium hydrogencarbonate T=80°C;
参考文献
Journal of the Chemical Society, , p. 376
反应条件
n-butyllithium; nitrobenzene 1.) THF, hexane, -75 deg C, 50 min.; 2.) -75 deg C, 4h, -> room temp.; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 48, # 12 p. 1941 - 1944
反应条件
n-butyllithium; nitrobenzene 1.) THF, hexane, -75 deg C, 50 min.; 2.) -75 deg C, 4h, -> room temp.; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 48, # 12 p. 1941 - 1944
反应条件
3-chloro-benzenecarboperoxoic acid; meso-tetra(2,6-dichloro-3-sulphonatophenyl)porphyrin iron chloride 2 h; Ambient temperature; Further byproducts given;
参考文献
Canadian Journal of Chemistry, , vol. 70, # 8 p. 2314 - 2318
反应条件
oxygen; anhydrous cobalt diacetate; acetic acid T=170°C; P=25857.4 Torr; 3 h; var. reaction partner systems; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 53, # 8 p. 1673 - 1679
