3,4-二甲氧基苯甲醛合成路线 （共 996 条）
参考文献
Dimmock; Nyathi; Smith
Journal of Pharmaceutical Sciences, 1979 , vol. 68, # 10 p. 1216 - 1221
反应条件
in ethanol
T=20°C; 5 h;
参考文献
Gududuru, Veeresa; Hurh, Eunju; Dalton, James T.; Miller, Duane D.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 7 p. 2584 - 2588
反应条件
lithium in tetrahydrofuran
T=-20°C;
参考文献
Shih, Neng-Yang; Mangiaracina, Pietro; Green, Michael J.; Ganguly, Ashit K.
Tetrahedron Letters, 1989 , vol. 30, # 41 p. 5563 - 5566
反应条件
antimony trichloride
T=120°C; 3 h; Neat (no solvent);
参考文献
Bardajee, Ghasem Rezanejade
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 135 - 144
反应条件
sodium hydroxide in methanol
10 h; Ambient temperature;
参考文献
Wattanasin, Sompong; Murphy, William S.
Synthesis, 1980 , # 8 p. 647 - 650
反应条件
potassium carbonate in methanol
van Leusen oxazole synthesis; 4 h; Heating;
参考文献
Besselievre, Francois; Mahuteau-Betzer, Florence; Grierson, David S.; Piguel, Sandrine
Journal of Organic Chemistry, 2008 , vol. 73, # 8 p. 3278 - 3280
反应条件
1: 99 percent / KOH / ethanol / 3 h / 20 °C
2: 90 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C
3: 97 percent / K2CO3 / acetone / 2 h / Heating
4: 86 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.5 h / 0 - 20 °C
5: 96 percent / K2CO3 / acetone / 1 h / Heating
6: 99 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C
7: 89 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.83 h / 0 - 20 °C
View Scheme
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
反应条件
Cu(II)-Mont K 10 clay in benzene
T=80°C; Condensation; 5 h;
参考文献
Phukan, Prodeep; Mohan, Jakkam Madan; Sudalai, Arumugam
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 24 p. 3685 - 3689
反应条件
sodium hydrogen sulphate; silica gel
T=58 - 60°C; 0.025 h; microwave irradiation;
参考文献
Gopalakrishnan, Mannathusamy; Sureshkumar, Purushothaman; Kanagarajan, Vijayakumar; Thanusu, Jeyaraman; Govindaraju, Ramalingam
Journal of Chemical Research, 2005 , # 5 p. 299 - 303
反应条件
1: aqueous-alcoholic NaOH-solution
2: platinum black; glacial acetic acid / Hydrogenation
View Scheme
参考文献
Pfeiffer et al.
Journal fuer Praktische Chemie (Leipzig), 1928 , vol. <2> 119, p. 120
