3,4-二甲氧基苯甲醛合成路线 （共 996 条）
反应条件
2: LAH
3: benzene / 0.75 h / Ambient temperature
4: 55.6 percent / FeSO4*7H2O, NH4OH / H2O / 3 h / Heating
5: 43.7 percent / 6 h / 154 °C
View Scheme
参考文献
Joshi; Chaudhari; Mogera
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 431 - 434
反应条件
1: 90 percent / piperidine / toluene / 110 °C
2: 84 percent / CHCl3; ethanol; H2O / 15 h / Heating
View Scheme
参考文献
White, James D.; Yager, Kraig M.; Yakura, Takayuki
Journal of the American Chemical Society, 1994 , vol. 116, # 5 p. 1831 - 1838
参考文献
Khalaji, Aliakbar Dehno; Grivani, Gholamhossein; Rezaei, Morteza; Fejfarova, Karla; Dusek, Michal
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 8 p. 1119 - 1126
反应条件
1: piperidine / 72 h / 30 - 40 °C
2: KOH / ethanol / Heating
3: polyphosphoric acid / Heating
4: zinc amalgam, aq. HCl / benzene / Heating
View Scheme
参考文献
Pramanik; Mukherjee
Journal of the Indian Chemical Society, 1997 , vol. 74, # 9 p. 734 - 735
反应条件
1: aq. NaOH
2: 84 percent / H2 / Pd/C / ethanol
View Scheme
参考文献
Ning, Xianling; Guo, Ying; Ma, Xiaoyan; Zhu, Renzong; Tian, Chao; Wang, Xiaowei; Ma, Zhizhong; Zhang, Zhili; Liu, Junyi
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 13 p. 3700 - 3703
反应条件
1: 74 percent / KCN / ethanol; H2O / 50 h / Heating
2: 33 percent / CuSO4*5H2O, pyridine / H2O / 7.67 h / Heating
3: 88 percent / aq. HBr, glacial acetic acid / 10 h / Heating
View Scheme
参考文献
Ohta, Kazuchika; Hasebe, Hiroshi; Ema, Hiroshi; Moriya, Mitsuo; Fujimoto, Tetsuya; Yamamoto, Iwao
Molecular Crystals and Liquid Crystals (1969-1991), 1991 , vol. 208, p. 21 - 32
反应条件
ammonium chloride in water; Petroleum ether
参考文献
Zhao, Xiumiao; Wan, Xiuying
Organic Preparations and Procedures International, 1995 , vol. 27, # 4 p. 513 - 516
反应条件
sodium disulfite in water
T=10°C; 0.666667 h;
参考文献
Jackson, W. Roy; Jacobs, Howard A.; Jayatilake, Gamini S.; Matthews, Barry R.; Watson, Keith G.
Australian Journal of Chemistry, 1990 , vol. 43, # 12 p. 2045 - 2062
参考文献
Buck
Journal of the American Chemical Society, 1933 , vol. 55, p. 2593,2594
反应条件
citrate buffer; prunus serotina leaves in di-isopropyl ether
T=20°C; 24 h; Title compound not separated from byproducts;
参考文献
Hernandez, Liliana; Luna, Hector; Solis, Aida; Vazquez, Alfredo
Tetrahedron Asymmetry, 2006 , vol. 17, # 19 p. 2813 - 2816
