3,4-二甲氧基苯甲醛合成路线 （共 996 条）
反应条件
1.1: potassium hydroxide / ethanol / 12 h / 0 - 20 °C
1.2: pH 3 - 4 / |Cooling with ice
2.1: Aspergillus niger LSPN001 / ethanol / 120 h / 20 °C / |Enzymatic reaction
View Scheme
参考文献
Alarcon, Julio; Alderete, Joel; Escobar, Carlos; Araya, Ramiro; Cespedes, Carlos L.
Biocatalysis and Biotransformation, 2013 , vol. 31, # 4 p. 160 - 167
参考文献
Davis,B.R.; Watkins,W.B.
Tetrahedron, 1968 , vol. 24, p. 2165 - 2175
反应条件
ethanol; N-benzyl-trimethylammonium hydroxide
参考文献
Walker
Journal of the American Chemical Society, 1955 , vol. 77, p. 3664,3666
反应条件
Yield given. Multistep reaction;
参考文献
Bubnov, Yu. N.; Gurskii, M. E.; Grandberg, A. I.; Pershin, D. G.
Tetrahedron, 1986 , vol. 42, # 4 p. 1079 - 1092
反应条件
in methanol; water
Ambient temperature;
参考文献
Badia, D.; Dominguez, E.; Galarza, J.; Lete, E.; Marigorta, E. Martinez de; Villa, M. J.
Bulletin des Societes Chimiques Belges, 1989 , vol. 98, # 1 p. 77 - 82
参考文献
Thies; Schoenenberger; el-Zanaty
Arzneimittel-Forschung, 1972 , vol. 22, # 7 p. 1138 - 1144
反应条件
(i) aq. Na2S2O5, (ii) /BRN= 3587243/; Multistep reaction;
参考文献
Crossley,R.; Curran,C.W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1974 , p. 2327 - 2330
参考文献
Rai, Mangat; Kaur, Baljit; Dhir, B. S.
Journal of the Indian Chemical Society, 1982 , vol. 59, # 3 p. 416 - 417
反应条件
magnesium sulfate in dichloromethane
T=20°C; 2 h;
参考文献
Cativiela; Falvello; Gines; Navarro; Urriolabeitia
New Journal of Chemistry, 2001 , vol. 25, # 2 p. 344 - 352
反应条件
1: piperidine / toluene / 110 °C
2: H2O / ethanol; CHCl3 / Heating
3: 44 percent / H2, aq. HCl / 10percent Pd/C / methanol / 22 h
View Scheme
参考文献
White, James D.; Yager, Kraig M.; Yakura, Takayuki
Journal of the American Chemical Society, 1994 , vol. 116, # 5 p. 1831 - 1838
