3,4-二甲氧基苯乙胺合成路线 （共 365 条）
反应条件
PPA in dichloromethane T=80°C; 72 h;
参考文献
Venkov, Atanas P.; Ivanov, Ilian I.
Tetrahedron, 1996 , vol. 52, # 37 p. 12299 - 12308
反应条件
toluene-4-sulfonic acid in toluene 3 h; Heating;
参考文献
Meyer, Horst
Liebigs Annalen der Chemie, 1981 , # 9 p. 1534 - 1544
反应条件
1: 2.) POCl3, P2O5 / 2.) xylene, reflux, 3 h 2: 54 percent / phosphoruspentasulphide / pyridine / 2.5 h / Heating 3: 60 percent / CH2Cl2 / 2 h / Heating View Scheme
参考文献
Sharma, S. D.; Mehra, Usha; Gupta, P. K.
Tetrahedron, 1980 , vol. 36, p. 3427 - 3430
反应条件
1: triethylamine / 1 h / 20 °C / |Inert atmosphere 2: boron tribromide / dichloromethane / 20 h / 0 - 20 °C View Scheme
参考文献
Fong, Hugo K.H.; Copp, Brent R.
Marine Drugs, 2013 , vol. 11, # 2 p. 274 - 299
反应条件
zirconium tetra-t-butoxide T=100°C; 0.25 h; microwave irradiation;
参考文献
Han, Chong; Porco Jr., John A.
Organic Letters, 2007 , vol. 9, # 8 p. 1517 - 1520
参考文献
Buck
Journal of the American Chemical Society, 1934 , vol. 56, p. 1607
反应条件
hydrogenchloride in water 6 h; Reflux;
参考文献
Marugan, Juan J.; Zheng, Wei; Motabar, Omid; Southall, Noel; Goldin, Ehud; Sidransky, Ellen; Aungst, Ronald A.; Liu, Ke; Sadhukhan, Subir Kumar; Austin, Christopher P.
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 5 p. 1880 - 1897
反应条件
1: NaNO2; aqueous acetic acid 2: tetrachloromethane; PCl5 View Scheme
参考文献
Buck
Journal of the American Chemical Society, 1931 , vol. 53, p. 2192,2195,2198
参考文献
Paytash et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 1415
反应条件
hydrogenchloride in chloroform
参考文献
Endo Laboratories
Patent: US4107165 A1, 1978 ;
