3,4-二甲氧基苯乙胺合成路线 （共 365 条）
参考文献
Buck; Perkin
Journal of the Chemical Society, 1924 , vol. 125, p. 1680
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Kitasato
Acta Phytochimica, 1927 , vol. 3, p. 253
Chem. Zentralbl., 1927 , vol. 98, # II p. 1966
参考文献
Buck; Perkin
Journal of the Chemical Society, 1924 , vol. 125, p. 1680
反应条件
tetrabutylammomium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in acetonitrile
T=20°C; 0.0833333 h; Inert atmosphereMolecular sieve;
参考文献
Drouet, Fleur; Fontaine, Patrice; Masson, Geraldine; Zhu, Jieping
Synthesis, 2009 , # 8 art. no. T19708SS, p. 1370 - 1374
反应条件
1: und Erwaermen des Reaktionsprodukts mit wss.Aethanol
2: aqueous hydriodic acid
View Scheme
参考文献
Kindler; Peschke
Archiv der Pharmazie (Weinheim, Germany), 1932 , vol. 270, p. 353,359
反应条件
1: molecular sieves 4 Angstroem / toluene / 12 h / Heating
2: NaBH4 / methanol / 0 - 20 °C
View Scheme
参考文献
Herrero, M.Teresa; Tellitu, Imanol; Dominguez, Esther; Hernandez, Susana; Moreno, Isabel; SanMartin, Raul
Tetrahedron, 2002 , vol. 58, # 42 p. 8581 - 8589
参考文献
Eilenberg, W.; Schaefer, H. J.
Tetrahedron Letters, 1984 , vol. 25, # 44 p. 5023 - 5026
反应条件
1.1: methanol
1.2: 175 - 178 °C
2.1: trichlorophosphate / benzene / 2 h / |Reflux
3.1: sodium tetrahydroborate; methanol / 0 - 5 °C
View Scheme
参考文献
Saidov; Alimova; Levkovich; Vinogradova
Chemistry of Natural Compounds, 2013 , vol. 49, # 2 p. 302 - 304
Khim. Prir. Soedin., 2013 , vol. 49, # 2 p. 257 - 258,2
反应条件
caesium carbonate
T=120°C;
参考文献
Jagtap, Sachin R.; Patil, Yogesh P.; Panda, Anil G.; Bhanage, Bhalchandra M.
Synthetic Communications, 2009 , vol. 39, # 12 p. 2093 - 2100
参考文献
Wiley et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 311
参考文献
Moyer; McEwen
Journal of the American Chemical Society, 1951 , vol. 73, p. 3075
