3,4-二甲氧基苯乙胺合成路线 （共 365 条）
参考文献
Buck
Journal of the American Chemical Society, 1931 , vol. 53, p. 2192,2195,2198
反应条件
sodium hydroxide in methanol; water; ethyl acetate; acetone
参考文献
Roussel UCLAF
Patent: US4175136 A1, 1979 ;
反应条件
methanol; palladium
Hydrogenation;
参考文献
Buth; Kuelz; Rosenmund
Chemische Berichte, 1939 , vol. 72, p. 19,28
反应条件
dihydrogen peroxide; iodine in water; dimethyl sulfoxide
T=110°C;
参考文献
Zhu, Yan-Ping; Liu, Mei-Cai; Cai, Qun; Jia, Feng-Cheng; Wu, An-Xin
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10132 - 10137
反应条件
1.1: potassium phosphate; sodium iodide / sulfolane / 20 - 35 °C / Inert atmosphere
1.2: 30 - 35 °C / Inert atmosphere
2.1: trichlorophosphate / 12 h / 80 °C / Inert atmosphere
3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 12 h / 25 °C
View Scheme
参考文献
Shankar; More, Satish S.; Madhubabu; Vembu; Syam Kumar
Synlett, 2012 , vol. 23, # 7 p. 1013 - 1020
