N,N-二乙基-4-氨基苯甲醛合成路线 (共 64 条)
反应条件
potassium tert-butylate Wittig reaction; Grinding;
参考文献
Zheng, Zheng; Zhou, Hong-Ping; Xu, Guo-Yi; Yu, Zhi-Peng; Yang, Xiao-Fei; Cheng, Long-Huai; Kong, Lin; Feng, Yan; Wu, Jie-Ying; Tian, Yu-Peng
Tetrahedron, 2012 , vol. 68, # 32 p. 6569 - 6574
参考文献
Gao, Fang; Ye, Xiaojuan; Li, Hongru; Zhong, Xiaolin; Wang, Qi
ChemPhysChem, 2012 , vol. 13, # 5 p. 1313 - 1324
反应条件
in tetrahydrofuran; dimethyl-ether T=-131°C; Kinetics; Further Variations:TemperaturesReaction partners;
参考文献
Jones, Amanda C.; Sanders, Aaron W.; Sikorski, William H.; Jansen, Kristin L.; Reich, Hans J.
Journal of the American Chemical Society, 2008 , vol. 130, # 19 p. 6060 - 6061
反应条件
acetic acid in toluene T=40 - 45°C; 3 h;
参考文献
Hodogaya Chemical Co., Ltd.
Patent: EP1762564 A1, 2007 ;
Location in patent: Page/Page column 7 ;
参考文献
Matsuoka, M.; Takao, M.; Kitao, T.; Fujiwara, T.; Nakatsu, K.
Molecular Crystals and Liquid Crystals (1969-1991), 1990 , vol. 182, p. 71 - 79
反应条件
Knoevenagel Condensation; Alkaline conditions;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 21, # 1 p. 135 - 145
参考文献
Sasaki, Takeo; Tachibana, Koji; Ono, Kazuo; Shimada, Teruyuki; Kudo, Masayuki; Katsuragi, Atsushi; Furuta, Toshiaki
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 368, p. 345 - 350
反应条件
sodium tris(acetoxy)borohydride in dichloromethane T=20°C; 18 h;
参考文献
Delarue; Girault; Maes; Debreu-Fontaine; Labaeid; Grellier; Sergheraert
Journal of Medicinal Chemistry, 2001 , vol. 44, # 17 p. 2827 - 2833
反应条件
piperidine in ethanol Knoevenagel condensation; Heating;
参考文献
Canadian Journal of Chemistry, , vol. 79, # 2 p. 174 - 182
反应条件
(i) NH2OH*HCl, Py, (ii) DCC, CuSO4*5H2O, Et3N; Multistep reaction;
参考文献
Vowinkel,E.; Bartel,J.
Chemische Berichte, 1974 , vol. 107, p. 1221 - 1227