1: (+/-)-α-(phenylthio)propanoic acid; benzoic acid anhydride With N-ethyl-N,N-diisopropylamine in deuterated toluene T=20°C; 0.0833333 h; Resolution of racemate; 2: benzyl alcohol With (S)-HBTM in deuterated toluene T=20°C; 24 h; Resolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Yang, Xing; Birman, Vladimir B.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 24 p. 5553 - 5555