反应条件
1.1: benzene / 4 h / Heating
2.1: LiAlH4; AlCl3 / tetrahydrofuran / 1 h / 0 °C
3.1: 83 percent / DIAD; Ph3P / benzene / 1 h / 20 °C
4.1: KOH / methanol / 0.17 h / 0 °C
4.2: 68 percent / methanol / 1 h / 0 °C
5.1: 94 percent / oxone / methanol; H2O / 0 °C
6.1: 84 percent / KOH; Al2O3; CBr2F2 / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Majewski, M.; Mpango, G. B.; Thomas, M. T.; Wu, A.; Snieckus, V.
Journal of Organic Chemistry, 1981 , vol. 46, # 10 p. 2029 - 2045
