1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 24.5 h / 0 - 130 °C
2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; tricyclo[3.3.1.13,7 ]-decane-1-carboxylic acid; potassium carbonate / m-xylene / 22 h / 120 °C / Inert atmosphere
3: sodium ethanolate / dimethyl sulfoxide / 24 h / 20 - 100 °C / Inert atmosphere
View Scheme
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Takazawa, Nobuo; Yamanaka, Hiroshi
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 16 p. 1927 - 1934