反应条件
1: 1.) n-butyllithium, 2.) I2 / 1.) THF, hexane, from -78 deg C to 20 deg C, 1 h, 2.) -78 deg C, 2 h 2: 1.) lithium diisopropylamide / 1.) THF, hexane, -78 deg C, 25 min, 2.) room temp., overnight 3: tert-butyllithium / tetrahydrofuran; pentane / 0.08 h / -100 °C 4: tetrahydrofuran / 6 h / -100 - 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 5 p. 757 - 761
