potassium hydroxide in water T=250°C; P=34200 - 38000 Torr; 12 h;
参考文献
Eryshev, B. Ya.; Smushkevich, Yu. I.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 4 p. 433 - 435
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , vol. 21, # 4 p. 519 - 521
1.1: trichlorophosphate / Cooling with ice 1.2: 2 h / 10 - 35 °C 1.3: Cooling with ice; Reflux 2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C 2.2: 2 h View Scheme
参考文献
Ismail, Mohamed A.H.; Abou El Ella, Dalal A.; Abouzid, Khaled A.M.; Mahmoud, Amr H.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 17 p. 5647 - 5647
Weiner, Wayne; Winkler, Jeffrey; Zimmerman, Steven C.; Czarnik, Anthony W.; Breslow, Ronald
Journal of the American Chemical Society, 1985 , vol. 107, # 13 p. 4093 - 4094
N+C3(R/S-DHBN)(S-Ala)2C16; N+C5(S-Ala)2C16; PL+C2N2C16; Cu(II) perchlorate in water T=30°C; 200 h; var. catalyst composition; Product distributionMechanism;
