反应条件
1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -70 °C / |Inert atmosphere
2.1: sec.-butyllithium / tetrahydrofuran; pentane / 1 h / -70 °C / |Inert atmosphere
2.2: 1 h / -70 °C / |Inert atmosphere
2.3: |Inert atmosphere
3.1: hydrogen; palladium 10 on activated carbon / methanol; chloroform / 12 h / 1810.07 Torr
View Scheme
参考文献
Bastos, Dayse Dos S.; Silva, Anna C.; Albert, Andre L.M.; Barros, Wesley M.R.; Slana, Glaucia B.C.A.; Cardoso, Jari N.; Lopes, Rosangela S.C.; Lopes, Claudio C.
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3144 - 3146