反应条件
n-butyl lithium in tetrahydrofuran; diethyl ether byproducts: LiCl; under N2, addn. of a soln. of n-Buli in hexane to soln. of benzothiazole in Et2O, addn. of soln. of triphenylstannylmethyliodide in THF to soln. of 2-lithiobenzothiazole in Et2O, stirring at -78 ° C for 1 h, warming up to room temp.; evapn., addn. of petroleum ether, filtration, TLC (silica, 1/1 ethyl acetate/80-100 petroleum ether);
参考文献
Journal of Organometallic Chemistry, , vol. 365, p. 61 - 74
