反应条件
1.1: potassium carbonate; potassium iodide / acetone / 48 h / 65 °C / Inert atmosphere
2.1: N-bromosuccinmide / tetrahydrofuran / Darkness
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 - 20 °C
3.2: 24 h / -78 - 20 °C
4.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / toluene / 0.67 h / 150 °C / Inert atmosphere; Microwave irradiation
View Scheme
参考文献
Zhao, Baomin; Liu, Bo; Png, Rui Qi; Zhang, Kai; Lim, Kheng Aik; Luo, Jing; Shao, Jinjun; Ho, Peter K.H.; Chi, Chunyan; Wu, Jishan
Chemistry of Materials, 2010 , vol. 22, # 2 p. 435 - 449