triethylamine in triethylamine
byproducts: triethylammonium chloride; under N2, GeCl4 added to stirred soln. of ligand (molar ratio 1:2) in Et3N at room temp., stirred for 1 h; Et3N evapd., treated with CHCl3, stirred, filtered under suction, residue treated with MeCN, heated under reflux, filtered hot, filtrate cooledto room temp.; elem. anal.;
参考文献
Sau, Arjun C.; Holmes, Robert R.
Inorganic Chemistry, 1981 , vol. 20, p. 4129 - 4135
Schuurmans, Norbert; Uji-i, Hiroshi; Mamdouh, Wael; De Schryver, Frans C.; Feringa, Ben L.; Van Esch, Jan; De Feyter, Steven
Journal of the American Chemical Society, 2004 , vol. 126, # 43 p. 13884 - 13885