反应条件
in tetrahydrofuran addn. of Grignard reagent to Co compound, standing (36 h, N2, Schlenk tube on a vac. line); vac. distn. (trapping in liquid N2), hydrolysed (aq. H2SO4), extd. (ether), filtn., org. layers are washed (aq. NaOH, water) and dried (MgSO4), sepn. of silane by chromy., aq. basic layers are acidified (aq. H2SO4), extd. (ether), evapn., yield catechol;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 42, p. 115 - 122
