Davitishvili, M. G.; Karpenko, R. G.; Malyutina, O. F.; Alekseeva, L. N.; Grinenko, G. S.
Pharmaceutical Chemistry Journal, 1988 , vol. 22, # 9 p. 716 - 720
Khimiko-Farmatsevticheskii Zhurnal, 1988 , vol. 22, # 9 p. 1121 - 1125
1: 88 percent / Jones reagent / acetone / 0.33 h / 0 - 5 °C
2: 1.) 10percent aq. HClO4, dibromantin, 2.) 10percent NaOH / 1.) acetone, 20 min, 2.) MeOH, 0-5 deg C, 1.5 h
3: HF, pyridine / 1 h / -78 °C
4: 72 percent / 15percent KOH / methanol; dioxane / 1.5 h / Heating
View Scheme
参考文献
Davitishvili, M. G.; Karpenko, R. G.; Malyutina, O. F.; Alekseeva, L. N.; Grinenko, G. S.
Pharmaceutical Chemistry Journal, 1988 , vol. 22, # 9 p. 716 - 720
Khimiko-Farmatsevticheskii Zhurnal, 1988 , vol. 22, # 9 p. 1121 - 1125
1: 88 percent / Jones reagent / acetone / 0.33 h / 0 - 5 °C
2: 1.) 10percent aq. HClO4, dibromantin, 2.) 10percent NaOH / 1.) acetone, 20 min, 2.) MeOH, 0-5 deg C, 1.5 h
3: HF, pyridine / 1 h / -78 °C
View Scheme
参考文献
Davitishvili, M. G.; Karpenko, R. G.; Malyutina, O. F.; Alekseeva, L. N.; Grinenko, G. S.
Pharmaceutical Chemistry Journal, 1988 , vol. 22, # 9 p. 716 - 720
Khimiko-Farmatsevticheskii Zhurnal, 1988 , vol. 22, # 9 p. 1121 - 1125
