4,5,7-O-三乙酰基-2,6-脱水-3-脱氧-D-来苏庚-2-烯腈合成路线 (共 5 条)
反应条件
pyridine; zinc in benzene 0.0833333 h; Heating;
参考文献
Somsak, Laszlo
Carbohydrate Research, 1990 , vol. 195, # 1 p. C1
反应条件
molecular sieve; 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane 20 h; Ambient temperature;
参考文献
Banaszek, Anna
Tetrahedron, 1995 , vol. 51, # 14 p. 4231 - 4238
反应条件
triethylamine; zinc in benzene Heatingeffect of additives on product yields; Product distribution;
参考文献
Journal of Carbohydrate Chemistry, , vol. 16, # 7 p. 1075 - 1087
反应条件
acetic acid Ambient temperatureother solvent: benzene, AcOH/water; other temperature: reflux; other additive: pyridine, triethylamine; Product distribution;
参考文献
Liebigs Annalen der Chemie, , # 12 p. 1265 - 1268
反应条件
sodium methylate T=20°C; Zemplen deacetylation; pH=8; 24 h;
参考文献
Somsak, Laszlo
Carbohydrate Research, 1996 , vol. 286, p. 167 - 171