5-乙氧基-4,5-二氢异噁唑-3-甲腈合成路线 （共 3 条）
反应条件
1: anti-N-hydroxy-2-(hydroxyimino)ethanimidoyl chloride With thionyl chloride in tetrahydrofuran T=0 - 15°C; Inert atmosphere; 2: ethyl vinyl ether With sodium carbonate in tetrahydrofuran; water T=0 - 5°C;
参考文献
Guohua, Jason; Hu, Weifeng; Liu, Renmao; Lu, Yuelie; Wu, Wenxue; Yang, Xiaogen
Patent: US2009/318705 A1, 2009 ;
Location in patent: Page/Page column 5 ;
反应条件
sodium carbonate in tetrahydrofuran; water T=0 - 5°C;
参考文献
Burgoon, Hugh Alfred; Buttar, Suzanne Marie; Frampton, Christopher Stephen
Patent: US2009/318516 A1, 2009 ;
Location in patent: Page/Page column 4-5 ;
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane T=0 - 5°C; Inert atmosphere;
参考文献
Burgoon, Hugh Alfred; Buttar, Suzanne Marie; Frampton, Christopher Stephen
Patent: US2009/318516 A1, 2009 ;
Location in patent: Page/Page column 5 ;
