N6-[叔丁氧羰基]-N2-[芴甲氧羰基]-2-甲基-L-赖氨酸合成路线 （共 7 条）
反应条件
sodium hydrogencarbonate in 1,4-dioxane; water T=0°C; 0.333333 h;
参考文献
Banerjee, Souvik; Wiggins, Walker J.; Geoghegan, Jessie L.; Anthony, Catherine T.; Woltering, Eugene A.; Masterson, Douglas S.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 37 p. 6307 - 6319
反应条件
sodium carbonate in 1,4-dioxane; water T=20°C;
参考文献
Chauhan, Satendra S.
Tetrahedron Letters, 2009 , vol. 50, # 49 p. 6913 - 6915
反应条件
1: pig liver esterase / aq. phosphate buffer; ethanol / pH 7.4 / |Enzymatic reaction 2: triethylamine; diphenyl phosphoryl azide / 1,2-dichloro-ethane / 5 h / 20 °C / |Inert atmosphere; |Reflux 3: titanium(IV) isopropylate / toluene / 12 h / 80 °C / |Inert atmosphere 4: hydrogenchloride / water; 1,4-dioxane / 24 h / |Reflux 5: sodium hydrogencarbonate / water; 1,4-dioxane / 0.33 h / 0 °C View Scheme
参考文献
Banerjee, Souvik; Wiggins, Walker J.; Geoghegan, Jessie L.; Anthony, Catherine T.; Woltering, Eugene A.; Masterson, Douglas S.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 37 p. 6307 - 6319
反应条件
1: triethylamine; diphenyl phosphoryl azide / 1,2-dichloro-ethane / 5 h / 20 °C / |Inert atmosphere; |Reflux 2: titanium(IV) isopropylate / toluene / 12 h / 80 °C / |Inert atmosphere 3: hydrogenchloride / water; 1,4-dioxane / 24 h / |Reflux 4: sodium hydrogencarbonate / water; 1,4-dioxane / 0.33 h / 0 °C View Scheme
参考文献
Banerjee, Souvik; Wiggins, Walker J.; Geoghegan, Jessie L.; Anthony, Catherine T.; Woltering, Eugene A.; Masterson, Douglas S.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 37 p. 6307 - 6319
反应条件
1: hydrogenchloride / water; 1,4-dioxane / 24 h / |Reflux 2: sodium hydrogencarbonate / water; 1,4-dioxane / 0.33 h / 0 °C View Scheme
参考文献
Banerjee, Souvik; Wiggins, Walker J.; Geoghegan, Jessie L.; Anthony, Catherine T.; Woltering, Eugene A.; Masterson, Douglas S.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 37 p. 6307 - 6319
反应条件
N-ethyl-N,N-diisopropylamine in 1,4-dioxane; water
参考文献
Chauhan, Satendra S.
Tetrahedron Letters, 2009 , vol. 50, # 49 p. 6913 - 6915
反应条件
1: C27H32N2O6 With palladium on activated charcoal; hydrogen 2: 1-[[(9H-fluoren-9-ylmethoxy)carbonyl]oxy]-2,5-pyrrolidinedione
参考文献
Zanuy, David; Sayago, Francisco J.; Revilla-Lopez, Guillem; Ballano, Gema; Agemy, Lilach; Kotamraju, Venkata Ramana; Jimenez, Ana I.; Cativiela, Carlos; Nussinov, Ruth; Sawvel, April M.; Stucky, Galen; Ruoslahti, Erkki; Aleman, Carlos
Journal of Computer-Aided Molecular Design, 2013 , vol. 27, # 1 p. 31 - 43
