magnesium iodide in diethyl ether
240 h; Ambient temperature;
参考文献
Hewkin, Cheryl T.; Jackson, Richard F. W.; Clegg, William
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3091 - 3102
Multi-step reaction with 2 steps 1: 92 percent / lithium tert-butyl hydroperoxide / tetrahydrofuran; toluene / a) -78 deg C, 10 min, b) -18 deg C, 55 min2: 72 percent / lithium iodide / acetone / 1 h / Heating
参考文献
Hewkin, Cheryl T.; Jackson, Richard F. W.; Clegg, William Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3091 - 3102
