反应条件
in neat (no solvent)
absence of air and moisture; molar ratio P4:S8=8:1, sealed tube (12 Torr), heating to 80°C; not isolated, reaction followed by (31)P-NMR spectroscopy;
参考文献
Jason, Mark E.; Ngo, Toan; Rahman, Shahidur
Inorganic Chemistry, 1997 , vol. 36, # 12 p. 2633 - 2640