2-溴-2',5'-二甲氧基苯乙酮合成路线 （共 16 条）
反应条件
copper(ll) bromide in chloroform; ethyl acetate 1.5 h; Heating;
参考文献
Sanchez-Viesca; Berros, Martha; Gomez
Heterocyclic Communications, 2003 , vol. 9, # 2 p. 165 - 170
反应条件
carbon disulfide; aluminium trichloride
参考文献
Chemische Berichte, , vol. 44, p. 3219
反应条件
1: acetone / 0.17 h / Heating 2: 2 N HBr / 1 h / Heating View Scheme
参考文献
Andreani; Rambaldi; Bonazzi; Bossa; Galatulas
Archiv der Pharmazie, 1985 , vol. 318, # 11 p. 1003 - 1008
反应条件
1: NaBH4 / dioxane; H2O / 1 h / Ambient temperature 2: KOH / diethyl ether; H2O / 0.5 h / Heating 3: NH3 / ethanol / 120 h / Ambient temperature View Scheme
参考文献
Epifani, E.; Lapucci, A.; Macchia, B.; Macchia, F.; Tognetti, P.; et al.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 2 p. 254 - 259
参考文献
Greiner,G. et al.
Chimica Therapeutica, 1966 , vol. 1, p. 408 - 414
反应条件
tetrabutylammomium bromide in water; toluene T=20°C; chemoselective reaction;
参考文献
Patil, Shivaraj P.; Kanawade, Shrikant B.; Shinde, Madhukar P.; Toche, Raghunath B.
Indian Journal of Heterocyclic Chemistry, 2011 , vol. 21, # 1 p. 33 - 36
反应条件
in 1,4-dioxane T=50°C; 0.5 h;
参考文献
Sanchez-Viesca; Berros, Martha; Gomez
Heterocyclic Communications, 2003 , vol. 9, # 2 p. 165 - 170
反应条件
1: 93 percent / benzene / 5 h / Ambient temperature 2: 49 percent / NaBH4, 2 N aq. NaOH / methanol / 1 h / Ambient temperature 3: 67 percent / H2 / 10percent Pd/C / ethanol / 50 °C / 760 Torr View Scheme
参考文献
Epifani, E.; Lapucci, A.; Macchia, B.; Macchia, F.; Tognetti, P.; et al.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 2 p. 254 - 259
反应条件
1: acetone / 0.17 h / Heating 2: 2 N HBr / 1 h / Heating View Scheme
参考文献
Andreani; Rambaldi; Bonazzi; Bossa; Galatulas
Archiv der Pharmazie, 1985 , vol. 318, # 11 p. 1003 - 1008
反应条件
ammonium chloride; zinc in ethanol T=80°C; 0.00833333 h; microwave irradiation;
参考文献
Li, Jian; Ye, Deju; Liu, Hong; Luo, Xiaoming; Jiang, Hualiang
Synthetic Communications, 2008 , vol. 38, # 4 p. 567 - 575
