2-溴-2',5'-二甲氧基苯乙酮合成路线 （共 16 条）
反应条件
pyridine T=10°C; Irradiation; Title compound not separated from byproducts;
参考文献
Chemistry Letters, , p. 33 - 36
反应条件
pyridine
T=10°C; Irradiation; Title compound not separated from byproducts;
参考文献
Izawa, Yasuji; Watoh, Yasushi; Tomioka, Hideo
Chemistry Letters, 1984 , p. 33 - 36
反应条件
hydrogenchloride; sodium hydroxide; dimethyl amine in water; toluene
参考文献
Ciba-Geigy Corporation
Patent: US4818765 A1, 1989 ;
参考文献
Bhattacharya,A.K.; Hortmann,A.G.
Journal of Organic Chemistry, 1974 , vol. 39, p. 95 - 99
反应条件
1: NaBH4 / dioxane; H2O / 1 h / Ambient temperature
2: KOH / diethyl ether; H2O / 0.5 h / Heating
3: NH3 / ethanol / 120 h / Ambient temperature
4: 50 percent / NaOH / CH2Cl2; H2O / 4 h / Ambient temperature
View Scheme
参考文献
Epifani, E.; Lapucci, A.; Macchia, B.; Macchia, F.; Tognetti, P.; et al.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 2 p. 254 - 259
反应条件
tetrabutylammomium bromide in water; toluene
T=20°C; chemoselective reaction;
参考文献
Patil, Shivaraj P.; Kanawade, Shrikant B.; Shinde, Madhukar P.; Toche, Raghunath B.
Indian Journal of Heterocyclic Chemistry, 2011 , vol. 21, # 1 p. 33 - 36
