4-甲基-联苯-4-胺盐酸盐合成路线 (共 29 条)
反应条件
nickel in ethanol; ethyl acetate T=65°C;
参考文献
Baltus, Christine B.; Press, Neil J.; Antonijevic, Milan D.; Tizzard, Graham J.; Coles, Simon J.; Spencer, John
Tetrahedron, 2012 , vol. 68, # 45 p. 9272 - 9277
反应条件
K3PO4*7H2O; palladium diacetate in water; N,N-dimethyl-formamide T=80°C; Suzuki Coupling; 0.333333 h;
参考文献
Tang, Wei; Yuan, Wei-Guan; Zhao, Bo; Zhang, Hong-Ling; Xiong, Fang; Jing, Lin-Hai; Qin, Da-Bin
Journal of Organometallic Chemistry, 2013 , vol. 743, p. 147 - 155
反应条件
tetrabutyl ammonium fluoride; potassium carbonate in water T=100°C; Suzuki-Miyaura coupling; 8 h;
参考文献
Yamada, Yoichi M. A.; Sarkar, Shaheen M.; Uozumi, Yasuhiro
Journal of the American Chemical Society, 2012 , vol. 134, # 6 p. 3190 - 3198
反应条件
potassium carbonate; palladium dichloride in PEG400; water T=20°C; Suzuki-Miyaura coupling; 0.25 h; Air atmosphere;
参考文献
Du, Zhengyin; Zhou, Wanwei; Wang, Fen; Wang, Jin-Xian
Tetrahedron, 2011 , vol. 67, # 26 p. 4914 - 4918
反应条件
palladium diacetate in water; N,N-dimethyl-formamide T=50°C; 5 h;
参考文献
Yamamoto, Yasunori; Takizawa, Miho; Yu, Xiao-Qiang; Miyaura, Norio
Angewandte Chemie - International Edition, 2008 , vol. 47, # 5 p. 928 - 931
反应条件
NiCl2[(4-MeOPh)3P]2; K3PO4*3H2O; tris(4-methoxyphenyl)-phosphine in toluene T=110°C; 10 h; Inert atmosphere;
参考文献
Chen, Xiaofeng; Ke, Haihua; Zou, Gang
ACS Catalysis, 2014 , vol. 4, # 2 p. 379 - 385
反应条件
1: copper powder / dimethylformamide / 6 h / Heating 2: H2 / Pd/C / ethanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 103, # 3 p. 645 - 653
反应条件
1: copper powder / dimethylformamide / 6 h / Heating 2: H2 / Pd/C / ethanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 103, # 3 p. 645 - 653
反应条件
10 palladium on activated charcoal; hydrogen in ethanol; ethyl acetate T=65°C;
参考文献
Spencer, John; Baltus, Christine B.; Press, Neil J.; Harrington, Ross W.; Clegg, William
Tetrahedron Letters, 2011 , vol. 52, # 31 p. 3963 - 3968
反应条件
10 palladium on activated charcoal; hydrogen in ethanol; ethyl acetate T=65°C;
参考文献
Spencer, John; Baltus, Christine B.; Press, Neil J.; Harrington, Ross W.; Clegg, William
Tetrahedron Letters, 2011 , vol. 52, # 31 p. 3963 - 3968