1: N,N-dimethyl-formamide With trichlorophosphate in 1,2-dichloro-ethane T=0°C; Inert atmosphere; 2: (4-morpholinyl)benzene in 1,2-dichloro-ethane Inert atmosphereReflux; 3: With triethylamine in 1,2-dichloro-ethane 24 h; Inert atmosphere;
参考文献
Wu, Chun; Dunaway-Mariano, Debra; Mariano, Patrick S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1910 - 1922