1: 92 percent / KOH / methanol / 3 h / Ambient temperature 2: 86 percent / propan-2-ol / 6 h / 80 °C 3: 100 percent / H2 / 10percent Pd/C / ethanol / 24 h View Scheme
参考文献
Parkes, Kevin E. B.; Bushnell, David J.; Crackett, Peter H.; Dunsdon, Stephen J.; Freeman, Andrew C.; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3656 - 3664
1: 92 percent / KOH / methanol / 3 h / Ambient temperature 2: 86 percent / propan-2-ol / 6 h / 80 °C 3: 100 percent / H2 / 10percent Pd/C / ethanol / 24 h 4: 48 percent / 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide, N-ethylmorpholine / tetrahydrofuran / 64 h / Ambient temperature 5: H2 / 10percent Pd/C / ethanol / 16 h 6: 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide, N-ethylmorpholine / tetrahydrofuran / 16 h / Ambient temperature View Scheme
参考文献
Parkes, Kevin E. B.; Bushnell, David J.; Crackett, Peter H.; Dunsdon, Stephen J.; Freeman, Andrew C.; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3656 - 3664
1: 92 percent / KOH / methanol / 3 h / Ambient temperature
2: 86 percent / propan-2-ol / 6 h / 80 °C
3: 100 percent / H2 / 10percent Pd/C / ethanol / 24 h
4: 48 percent / 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide, N-ethylmorpholine / tetrahydrofuran / 64 h / Ambient temperature
View Scheme
参考文献
Parkes, Kevin E. B.; Bushnell, David J.; Crackett, Peter H.; Dunsdon, Stephen J.; Freeman, Andrew C.; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3656 - 3664
