5-甲氧基-2-苯基-2H-吲唑合成路线 (共 11 条)
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; sodium t-butanolate in toluene T=90°C; Cyclization; Aromatization; 15 h;
参考文献
Song; Yee
Organic letters, 2000 , vol. 2, # 4 p. 519 - 521
反应条件
N-doped TiO2 in water T=20°C; 3 h; UV-irradiationInert atmosphere;
参考文献
Selvam; Balachandran; Velmurugan; Swaminathan
Applied Catalysis A: General, 2012 , vol. 413-414, p. 213 - 222
反应条件
N-doped TiO2 in water T=20°C; 3 h; UV-irradiationInert atmosphere;
参考文献
Selvam; Balachandran; Velmurugan; Swaminathan
Applied Catalysis A: General, 2012 , vol. 413-414, p. 213 - 222
反应条件
N-doped TiO2 in water T=20°C; 3 h; sunlightInert atmosphere;
参考文献
Selvam; Balachandran; Velmurugan; Swaminathan
Applied Catalysis A: General, 2012 , vol. 413-414, p. 213 - 222
反应条件
N-doped TiO2 in water T=20°C; 3 h; sunlightInert atmosphere;
参考文献
Selvam; Balachandran; Velmurugan; Swaminathan
Applied Catalysis A: General, 2012 , vol. 413-414, p. 213 - 222
反应条件
1.1: NaHMDS / tetrahydrofuran / 0 - 20 °C 1.2: tetrahydrofuran / 20 °C 2.1: 60 percent / Pd(OAc)2; dppf; t-BuONa / toluene / 15 h / 90 °C View Scheme
参考文献
Song; Yee
Organic letters, 2000 , vol. 2, # 4 p. 519 - 521
反应条件
1.1: NaHMDS / tetrahydrofuran / 0 - 20 °C 1.2: tetrahydrofuran / 20 °C 2.1: 60 percent / Pd(OAc)2; dppf; t-BuONa / toluene / 15 h / 90 °C View Scheme
参考文献
Song; Yee
Organic letters, 2000 , vol. 2, # 4 p. 519 - 521
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 12 h;
参考文献
Fang, Yuesi; Wu, Chunrui; Larock, Richard C.; Shi, Feng
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 8840 - 8851
反应条件
Titanium(IV) oxide in methanol 6 h; Irradiation;
参考文献
Shibata, Katsuyoshi; Mimura, Tadashi; Matsui, Masaki; Sugiura, Takashi; Minoura, Hideki
Journal of the Chemical Society, Chemical Communications, 1988 , # 19 p. 1318 - 1320
反应条件
1: sodium nitrite / water / 0.33 h / 0 °C 2: acetic anhydride / 5 h / 100 °C 3: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 20 °C View Scheme
参考文献
Fang, Yuesi; Wu, Chunrui; Larock, Richard C.; Shi, Feng
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 8840 - 8851