4-碘-2,6-二(羟基甲基)吡啶合成路线 （共 5 条）
反应条件
sodium tetrahydroborate in methanol 17 h; Heating;
参考文献
Storm, Ole; Luening, Ulrich
European Journal of Organic Chemistry, 2002 , # 21 p. 3680 - 3685
反应条件
sodium tetrahydroborate in ethanol
参考文献
Takalo, Harri; Pasanen, Paavo; Kankare, Jouko
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1988 , vol. 42, # 6 p. 373 - 377
反应条件
1: 90 percent / hydrogen iodide; phosphorous acid / 5 h / Heating 2: 70 percent / sulfuric acid / 4 h / Heating 3: 70 percent / sodium borohydride / methanol / 17 h / Heating View Scheme
参考文献
Gilday, Lydia C.; Lang, Thomas; Caballero, Antonio; Costa, Paulo J.; Felix, Vitor; Beer, Paul D.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 16 p. 4356 - 4360
Angew. Chem., 2013 , vol. 125, # 16 p. 4452 - 4456
反应条件
phosphorus tribromide in N,N-dimethyl-formamide T=0 - 20°C; 4 h;
参考文献
DHR Finland OY; Meltola, Niko; Takalo, Harri; Sund, Henri
Patent: US2013/183771 A1, 2013 ;
Location in patent: Paragraph 0093; 0094 ;
反应条件
selenium(IV) oxide in 1,4-dioxane
5.5 h; Heating;
参考文献
Storm, Ole; Luening, Ulrich
European Journal of Organic Chemistry, 2002 , # 21 p. 3680 - 3685
