3-(溴甲基)-5-甲基苯甲酸甲酯合成路线 (共 3 条)
反应条件
Sodium bromate; sodium hydrogensulfite in water; ethyl acetate T=20°C; 4 h;
参考文献
Jackson, Toby; Woo, L. W. Lawrence; Trusselle, Melanie N.; Chander, Surinder K.; Purohit, Atul; Reed, Michael J.; Potter, Barry V. L.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 18 p. 2940 - 2952
反应条件
Sodium bromate; potassium hydrogensulfate in water; ethyl acetate T=20°C; 5 h; Product distribution / selectivity;
参考文献
KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY; KIM, Choung, U.; MITCHELL, Michael, L.; SON, Jong, Chan
Patent: WO2010/9047 A1, 2010 ;
Location in patent: Page/Page column 74 ;
WO 2010/009047 A1
反应条件
1: SOCl2 2: 25 percent / NBS, AIBN / methyl formate View Scheme
参考文献
Loewik, Dennis W. P. M.; Weingarten, W. David; Broekema, Matthias; Brouwer, Arwin J.; Still, W. Clark; Liskamp, Rob M. J.
Angewandte Chemie - International Edition, 1998 , vol. 37, # 13-14 p. 1846 - 1850