2-丙炔-1-基氨基甲酸苄酯合成路线 (共 6 条)
反应条件
sodium hydrogencarbonate in ethanol; water T=0 - 20°C; 14 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 28 p. 7764 - 7767
反应条件
sodium hydrogencarbonate in pyridine; dichloromethane; ethyl acetate
反应条件
in dichloromethane 0 deg C, 30 min then r.t.;
参考文献
Synthesis, , # 3 p. 276 - 284
反应条件
in dichloromethane T=0 - 20°C;
参考文献
Synlett, , # 15 p. 2314 - 2318
反应条件
hydrogen; palladium on activated charcoal; ethylenediamine in methanol-d4 T=20°C; Hydrogenation; 1 h;
参考文献
Hattori, Kazuyuki; Sajiki, Hironao; Hirota, Kosaku
Tetrahedron, 2000 , vol. 56, # 43 p. 8433 - 8441
反应条件
hydrogen; palladium on activated charcoal; ethylenediamine in tetrahydrofuran T=20°C; Hydrogenation; Product distribution; Further Variations:Solvents;
参考文献
Hattori, Kazuyuki; Sajiki, Hironao; Hirota, Kosaku
Tetrahedron, 2000 , vol. 56, # 43 p. 8433 - 8441