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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
120586-28-9
合成路线
（共 5 条）
120586-28-9
→
反应条件
40983-58-2
甲基(-)-莽草酸
反应条件
1: 95 percent / lithium aluminium hydride / diethyl ether / Ambient temperature 2: 45 percent / Raney Ni (W-2) / ethanol / Ambient temperature 3: Jones reagent / acetone / Ambient temperature 4: diethyl ether; methanol 5: 56 percent / lithium hexamethyldisilazide / tetrahydrofuran / -78 °C 6: trimethylsilyl chloride, sodium iodide / acetonitrile / Ambient temperature View Scheme
参考文献
Takahashi, Tamiko; Namiki, Toshie; Takeuchi, Yoshio; Koizumi, Toru
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 8 p. 3213 - 3215
120586-28-9
→
反应条件
120586-29-0
反应条件
With lithium aluminium tetrahydride in diethyl ether 0.916667 h; Ambient temperature;
参考文献
Takahashi, Tamiko; Kotsubo, Hironori; Iyobe, Akira; Namiki, Toshie; Koizumi, Toru Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 3065 - 3072
120586-28-9
→
反应条件
120586-30-3
反应条件
Multi-step reaction with 2 steps 1: 95 percent / LiAlH4 / diethyl ether / 0.92 h / Ambient temperature2: 45 percent / Raney Ni (W-2) / ethanol / 144 h / Ambient temperature
参考文献
Takahashi, Tamiko; Kotsubo, Hironori; Iyobe, Akira; Namiki, Toshie; Koizumi, Toru Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 3065 - 3072
120586-28-9
→
反应条件
120586-31-4
反应条件
Multi-step reaction with 4 steps 1: 95 percent / LiAlH4 / diethyl ether / 0.92 h / Ambient temperature2: 45 percent / Raney Ni (W-2) / ethanol / 144 h / Ambient temperature3: Jones reagent / acetone / 2.5 h / Ambient temperature4: methanol / 0.83 h / 0 °C
参考文献
Takahashi, Tamiko; Kotsubo, Hironori; Iyobe, Akira; Namiki, Toshie; Koizumi, Toru Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 3065 - 3072
120586-28-9
→
反应条件
120586-32-5
反应条件
Multi-step reaction with 5 steps 1: 95 percent / LiAlH4 / diethyl ether / 0.92 h / Ambient temperature2: 45 percent / Raney Ni (W-2) / ethanol / 144 h / Ambient temperature3: Jones reagent / acetone / 2.5 h / Ambient temperature4: methanol / 0.83 h / 0 °C5: 56 percent / BuLi, hexamethyldisilazane / hexane; tetrahydrofuran / 0.5 h / -78 °C
参考文献
Takahashi, Tamiko; Kotsubo, Hironori; Iyobe, Akira; Namiki, Toshie; Koizumi, Toru Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 3065 - 3072
