3,6-二甲氧基-2-硝基苯甲醛合成路线 （共 14 条）
反应条件
nitric acid; silica gel
参考文献
Synlett, , # 9 p. 1431 - 1434
反应条件
hydrogenchloride; nitric acid 1.) acetic anhydride, from 10 deg C to 15 deg C, 1 h, 2.) acetic anhydride, 2 h; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 22, # 14 p. 2071 - 2076
反应条件
cerium(IV) ammonium nitrate supported on silica in dichloromethane 0.25 h;
参考文献
Tetrahedron Letters, , vol. 33, # 27 p. 3855 - 3858
反应条件
nitric acid Ambient temperature;
参考文献
Journal of Medicinal Chemistry, , vol. 29, # 8 p. 1329 - 1340
反应条件
nitric acid; acetic acid in diethyl ether 30 h; Ambient temperature;
参考文献
Synthetic Communications, , vol. 23, # 10 p. 1351 - 1356
参考文献
Medicinal Chemistry Research, , vol. 9, # 6 p. 374 - 388
参考文献
Journal of the Chemical Society, , vol. 127, p. 2003
反应条件
1: AcOH; NaOAc / 5 h / Heating 2: H2; HCOONH4 / Pd/C / ethanol / 0.5 h / Heating View Scheme
参考文献
Showalter, H. D. Hollis; Pohlmann, Gerd
Organic Preparations and Procedures International, 1992 , vol. 24, # 4 p. 484 - 488
反应条件
hydrogen; palladium on activated charcoal in methanol P=1810.02 Torr; 6 h; Ambient temperature;
参考文献
Blanco, Ma del Mar; Avendano, Carmen; Cabezas, Nieves; Menendez, J. Carlos
Heterocycles, 1993 , vol. 36, # 6 p. 1387 - 1398
反应条件
1: 76 percent / Fe, conc. HCl / ethanol; acetic acid; H2O / 0.25 h / Heating 2: 75 percent / KOH / ethanol / 18 h / Heating 3: 85 percent / ceric ammonium nitrate, pyridine-2,6-dicarboxylic acid N-oxide / acetonitrile; H2O / 1.) 0 deg C, 30 min, 2.) 20 deg C, 30 min View Scheme
参考文献
Thummel, Randolph P.; Chirayil, Sara; Hery, Christophe; Lim, Jean-Luc; Wang, Tie-Lin
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1666 - 1671
