Kini, Ganesh D.; Henry, Elizabeth M.; Robins, Roland K.; Larson, Steven B.; Marr, J. Joseph; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 44 - 48
1: 58 percent / 70percent perchloric acid / acetone / 1.5 h / 0 °C 2: 1.) NaH / 1.) THF, 0 deg C, 15 min, 2.) a.) 0 deg C, 2 h, b.) RT, 4 h 3: 93 percent / 80percent acetic acid / 2 h / 100 °C View Scheme
参考文献
Kini, Ganesh D.; Henry, Elizabeth M.; Robins, Roland K.; Larson, Steven B.; Marr, J. Joseph; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 44 - 48
1: 1.) NaH / 1.) THF, 0 deg C, 15 min, 2.) a.) 0 deg C, 2 h, b.) RT, 4 h 2: 93 percent / 80percent acetic acid / 2 h / 100 °C View Scheme
参考文献
Kini, Ganesh D.; Henry, Elizabeth M.; Robins, Roland K.; Larson, Steven B.; Marr, J. Joseph; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 44 - 48
